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Beilstein J. Nanotechnol. 2014, 5, 760–769, doi:10.3762/bjnano.5.88
Figure 1: GC profile of the products formed during CO2 hydrogenation at different temperatures.
Figure 2: TEM and HRTEM of Fe/Fe3O4 nanoparticles prepared by thermal decomposition of Fe(CO)5 in the presenc...
Figure 3: TEM and HRTEM of Fe/Fe3O4 nanoparticles prepared by thermal decomposition of Fe(CO)5 in the presenc...
Figure 4: XRD patterns of the Fe/Fe3O4 nanoparticles as a function of catalytic run (2 h at 400 °C).
Figure 5: XPS surveys of the catalyst: a) as prepared with HDA synthesis, b) after 5 runs, c) after 10 runs, ...
Figure 6: XPS of the Fe 2p3/2 and Fe 2p1/2 region for the catalyst: a) after 10 runs, b) after 5 runs, c) as ...
Scheme 1: Hydrogenation of carbon suboxide.
Scheme 2: Trimerization of hydrogenated carbon suboxide on Fe3O4.
Scheme 3: Keto–enol tautomerism leads to aromatization.
Scheme 4: Reduction of the intermediate phenol derivative to mesitylene.
Scheme 5: Demethylation is at this stage of mechanistic research the most likely process explaining the forma...
Figure 7: Product selectivities as a function of temperature: blue: 440 °C, yellow: 480 °C, orange: 500 °C, r...
Figure 8: Tubular reactor used in the catalytic reduction reaction.